2-Methoxy-5-nitrobenzoic acid 2-[[[2,7-bis(1,1-dimethylethyl)-9H-fluoren-9-yl]methoxy]carbonyl]hydrazide

Base Information

Chemical Name:2-Methoxy-5-nitrobenzoic acid 2-[[[2,7-bis(1,1-dimethylethyl)-9H-fluoren-9-yl]methoxy]carbonyl]hydrazide
CAS No.:287381-48-0
Molecular Formula:C₃₁H₃₅N₃O₆
Molecular Weight:545.635
Hs Code.:
DSSTox Substance ID:DTXSID701111394
Nikkaji Number:J1.374.011I

Synonyms:DTXSID701111394;2-Methoxy-5-nitrobenzoic acid 2-[[[2,7-bis(1,1-dimethylethyl)-9H-fluoren-9-yl]methoxy]carbonyl]hydrazide;287381-48-0

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methoxy-5-nitrobenzoic acid 2-[[[2,7-bis(1,1-dimethylethyl)-9H-fluoren-9-yl]methoxy]carbonyl]hydrazide

Chemical Property:

XLogP3:7.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:7
Exact Mass:545.25258584
Heavy Atom Count:40
Complexity:884

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)C1=CC2=C(C=C1)C3=C(C2COC(=O)NNC(=O)C4=C(C=CC(=C4)[N+](=O)[O-])OC)C=C(C=C3)C(C)(C)C

Technology Process of 2-Methoxy-5-nitrobenzoic acid 2-[[[2,7-bis(1,1-dimethylethyl)-9H-fluoren-9-yl]methoxy]carbonyl]hydrazide

There total 2 articles about 2-Methoxy-5-nitrobenzoic acid 2-[[[2,7-bis(1,1-dimethylethyl)-9H-fluoren-9-yl]methoxy]carbonyl]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 287381-46-8
2,7-di-tert-butyl-9-fluorenylmethoxycarbonyl chloride

: 287381-48-0
N'-(2-methoxy-5-nitro-benzoyl)-hydrazinecarboxylic acid 2,7-di-tert-butyl-9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / hydrazine / diethyl ether / 3 h

2: pyridine / CH₂Cl₂ / 0.5 h

With pyridine; hydrazine; In diethyl ether; dichloromethane; 1: Acylation / 2: Acylation;
DOI:10.1021/ja001142w