4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate

Base Information

Chemical Name:4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate
CAS No.:98304-00-8
Molecular Formula:C₂₃H₂₁F₁₂N₅O₄P₃*C₂₄H₂₀B
Molecular Weight:1071.59
Hs Code.:

4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro<phenaleno<1,9-de>-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate

Synonyms:4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate

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Chemical Property of 4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate

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Technology Process of 4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate

There total 3 articles about 4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98304-01-9
9-amino-1-methyliminophenalene

: 98304-00-8
4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / diisopropylethylamine, hexachlorocyclotriphosphazene / dioxane / Heating

2: 69 percent / tetrahydrofuran

3: 1.) nitromethane, 15 min; 2.) methanol, reflux

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ja00311a061

Reference yield:

: 98330-18-8
4',4',6',6'-tetrachloro-4',4',6',6'-tetrahydro-1-methylspiro-1,3,2-diazaphosphorine-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine>

: 98304-00-8
4',4',6',6'-tetrakis(trifluoroethoxy)-4',4',6',6'-terahydro-1,3-dimethylspiro-1,3,2-diazaphosphorinium-2(1H),2'-<1,3,5,2,4,6>triazatriphosphorine> tetraphenylborate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / tetrahydrofuran

2: 1.) nitromethane, 15 min; 2.) methanol, reflux

In tetrahydrofuran;
DOI:10.1021/ja00311a061