C₆₃H₉₆F₂N₁₀O₉

Base Information

Chemical Name:C₆₃H₉₆F₂N₁₀O₉
CAS No.:1519003-80-5
Molecular Formula:C₆₃H₉₆F₂N₁₀O₉
Molecular Weight:1175.51
Hs Code.:

C<sub>63</sub>H<sub>96</sub>F<sub>2</sub>N<sub>10</sub>O<sub>9</sub>

Synonyms:C₆₃H₉₆F₂N₁₀O₉

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Chemical Property of C₆₃H₉₆F₂N₁₀O₉

Chemical Property:

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Technology Process of C₆₃H₉₆F₂N₁₀O₉

There total 19 articles about C₆₃H₉₆F₂N₁₀O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1519003-77-0
C₃₆H₅₄F₂N₈O

: 1519003-86-1
C₂₇H₄₂N₂O₈

: 1519003-80-5
C₆₃H₉₆F₂N₁₀O₉

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; 3-[4-[[bis[[1-(3-hydroxypropyl)triazol-4-yl]methyl]amino]methyl]triazol-1-yl]propan-1-ol; In tert-butyl alcohol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ml400370w

Reference yield:

: 76272-34-9
8-Benzyl-1αH,5αH-nortropan-3-one Oxime

: 1519003-80-5
C₆₃H₉₆F₂N₁₀O₉

Guidance literature:: Multi-step reaction with 14 steps

1: sodium; propan-1-ol / toluene / 12 h / Reflux; Inert atmosphere

2: tetrahydrofuran / 72 h / 20 °C / Inert atmosphere

3: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

5: phosphorus pentachloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

6: dichloromethane; tert-Amyl alcohol / 0 - 20 °C / Inert atmosphere

7: acetic acid / ethyl acetate / 0.5 h / 80 °C / Inert atmosphere

8: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 2585.81 Torr / Inert atmosphere

9: hydrogen bromide / 2 h / 100 °C / Inert atmosphere

10: sodium hydroxide / water; dichloromethane / 20 °C / pH 12 / Inert atmosphere

11: sodium azide / ethanol / 4 h / 100 °C / Inert atmosphere

12: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

13: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 3 h / 20 °C / Inert atmosphere

14: 3-[4-[[bis[[1-(3-hydroxypropyl)triazol-4-yl]methyl]amino]methyl]triazol-1-yl]propan-1-ol; copper(II) sulfate; sodium L-ascorbate / tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; propan-1-ol; sodium azide; phosphorus pentachloride; palladium 10% on activated carbon; hydrogen bromide; hydrogen; sodium; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; copper(II) sulfate; acetic acid; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; 3-[4-[[bis[[1-(3-hydroxypropyl)triazol-4-yl]methyl]amino]methyl]triazol-1-yl]propan-1-ol; In tetrahydrofuran; 1,4-dioxane; methanol; tert-Amyl alcohol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/ml400370w

Reference yield:

: 8-benzyl-8-azabicyclo[3.2.1]octan-3-amine

: 1519003-80-5
C₆₃H₉₆F₂N₁₀O₉

Guidance literature:: Multi-step reaction with 13 steps

1: tetrahydrofuran / 72 h / 20 °C / Inert atmosphere

2: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4: phosphorus pentachloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5: dichloromethane; tert-Amyl alcohol / 0 - 20 °C / Inert atmosphere

6: acetic acid / ethyl acetate / 0.5 h / 80 °C / Inert atmosphere

7: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 2585.81 Torr / Inert atmosphere

8: hydrogen bromide / 2 h / 100 °C / Inert atmosphere

9: sodium hydroxide / water; dichloromethane / 20 °C / pH 12 / Inert atmosphere

10: sodium azide / ethanol / 4 h / 100 °C / Inert atmosphere

11: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere

12: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 3 h / 20 °C / Inert atmosphere

13: 3-[4-[[bis[[1-(3-hydroxypropyl)triazol-4-yl]methyl]amino]methyl]triazol-1-yl]propan-1-ol; copper(II) sulfate; sodium L-ascorbate / tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium azide; phosphorus pentachloride; palladium 10% on activated carbon; hydrogen bromide; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; copper(II) sulfate; acetic acid; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; 3-[4-[[bis[[1-(3-hydroxypropyl)triazol-4-yl]methyl]amino]methyl]triazol-1-yl]propan-1-ol; In tetrahydrofuran; 1,4-dioxane; methanol; tert-Amyl alcohol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ml400370w