5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin

Base Information

Chemical Name:5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin
CAS No.:98875-79-7
Molecular Formula:C₅₆H₄₇N₅O₂
Molecular Weight:822.021
Hs Code.:

Synonyms:5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin

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Chemical Property of 5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin

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Technology Process of 5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin

There total 2 articles about 5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 57412-07-4
5-(2-hydroxyphenyl)-10,15,20-tris(4-methylphenyl) porphyrin

: 98875-78-6
3-<(3-Chloropropoxy)methyl>pyridine

: 98875-79-7
5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 16h; Ambient temperature;
DOI:10.1021/jo00224a048

Reference yield:

: 6959-48-4
3-chloromethylpyridinium chloride

: 98875-79-7
5-<2-<3-(pyrid-3-ylmethoxy)propoxy>phenyl>-10,15,20-tri-p-tolylporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium tert-butoxide / 1.) THF, RT, 1 h, 2.) THF, a) RT, 48 h, b) reflux, 20 h

2: 85 percent / K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

With potassium tert-butylate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jo00224a048