2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline

Base Information

• Chemical Name: 2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline
• CAS No.: 1046790-54-8
• Molecular Formula: C₂₁H₂₃F₃N₆O₃
• Molecular Weight: 464.447

Synonyms:2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline

Chemical Property of 2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline

Chemical Property:

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Technology Process of 2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline

There total 1 articles about 2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(piperazin-1-yl)-2-(trifluoromethyl)-1H-benzo[d]imidazole (282547-72-2) + 2-(3-chloropropoxy)-6-nitroaniline (70282-36-9) → 2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline (1046790-54-8)

Guidance literature:

With triethylamine; In dimethyl sulfoxide; at 90 ℃; for 20h;

DOI:10.1016/j.bmc.2008.05.024

Reference yield:

2-nitro-6-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)aniline (1046790-54-8) → 3-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)benzene-1,2-diamine (1046790-57-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 18h; under 760.051 Torr;

DOI:10.1016/j.bmc.2008.05.024

upstream raw materials:

4-(piperazin-1-yl)-2-(trifluoromethyl)-1H-benzo[d]imidazole

2-(3-chloropropoxy)-6-nitroaniline

Downstream raw materials:

3-(3-{4-[2-(trifluoromethyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}propoxy)benzene-1,2-diamine

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