(1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

Base Information

Chemical Name:(1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide
CAS No.:464893-65-0
Molecular Formula:C₁₆H₂₁NO₂Se
Molecular Weight:338.308
Hs Code.:

Synonyms:(1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

Suppliers and Price of (1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

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Chemical Property of (1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

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Technology Process of (1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

There total 3 articles about (1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2179-79-5
phenyl selenocyanate

: 464893-60-5
(1S,2S,6R,7R)-2-hydroxy-N-methoxy-N-methylbicyclo[4.1.0]heptane-7-carboxamide

: 464893-65-0
(1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

Guidance literature:: With tributylphosphine; In tetrahydrofuran; for 14h; Heating;
DOI:10.1016/S0957-4166(02)00105-2

Reference yield:

: 123826-91-5
2-cyclohexen-1-yl diazoacetate

: 464893-65-0
(1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: [Rh₂{(2S)-meox}4] / CH₂Cl₂ / 15 h / 20 °C

2: 95 percent / AlMe₃ / heptane; CH₂Cl₂

3: 88 percent / Bu₃P / tetrahydrofuran / 14 h / Heating

With tributylphosphine; [Rh₂{(2S)-meox}4]; trimethylaluminum; In tetrahydrofuran; n-heptane; dichloromethane;
DOI:10.1016/S0957-4166(02)00105-2

Reference yield:

: 172722-65-5
(1S,2R,6S,9R)-(-)-7-oxatricyclo[4.3.0.0^2,9]nonan-8-one

: 464893-65-0
(1S,2R,6R,7R)-N-methoxy-N-methyl-2-phenylseleno bicyclo[4.1.0]heptane-7-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / AlMe₃ / heptane; CH₂Cl₂

2: 88 percent / Bu₃P / tetrahydrofuran / 14 h / Heating

With tributylphosphine; trimethylaluminum; In tetrahydrofuran; n-heptane; dichloromethane;
DOI:10.1016/S0957-4166(02)00105-2