Technology Process of Ti(N(phenyl)(4,4'-di-tert-butyl-2,2'-bipyridine)(N,N-di(pyrrolyl-α-methyl)-N-methylamine)
There total 1 articles about Ti(N(phenyl)(4,4'-di-tert-butyl-2,2'-bipyridine)(N,N-di(pyrrolyl-α-methyl)-N-methylamine) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
diethyl ether;
N2; soln. of aniline in Et2O added dropwise to nearly frozen soln. of Ticomplex and bipyridine deriv. in Et2O, stirring at room temp. overnight; volatiles removed under vac., recrystn. from CH2Cl2; elem. anal.;
DOI:10.1021/ja038320g