6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine

Base Information

Chemical Name:6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine
CAS No.:1006726-20-0
Molecular Formula:C₂₇H₃₀N₆O₅S
Molecular Weight:550.638
Hs Code.:

Synonyms:6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine

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Chemical Property of 6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine

Chemical Property:

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Technology Process of 6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine

There total 6 articles about 6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1006726-14-2
N-(2-pivaloyloxyethyl)-N-(pivaloyloxymethyl)-p-toluenesulfonamide

: 4005-49-6
N-benzoyladenine

: 1006726-20-0
6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine

: 1006726-21-1
6-benzoylamino-7-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-7H-purine

Guidance literature:: N-benzoyladenine; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 20 ℃; for 1h;

N-(2-pivaloyloxyethyl)-N-(pivaloyloxymethyl)-p-toluenesulfonamide; With tin(IV) chloride; In acetonitrile; at 20 ℃; for 72h; Further stages.;
DOI:10.1080/15257770601052281

Reference yield: 16.0%

: 1006726-21-1
6-benzoylamino-7-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-7H-purine

: 1006726-20-0
6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In toluene; at 80 ℃; for 2h;
DOI:10.1080/15257770601052281

Reference yield:

: 1006726-12-0
N-(2-pivaloyloxyethyl)-p-toluenesulfonamide

: 1006726-20-0
6-benzoylamino-9-[N-(2-pivaloyloxyethyl)-p-toluenesulfonylaminomethyl]-9H-purine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / dimethylformamide / 120 h / 20 °C

2.1: N,O-bis(trimethylsilyl)acetamide / acetonitrile / 1 h / 20 °C

2.2: 31 percent / SnCl₄ / acetonitrile / 72 h / 20 °C

With N,O-bis-(trimethylsilyl)-acetamide; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/15257770601052281