2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

Base Information

• Chemical Name: 2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one
• CAS No.: 96017-31-1
• Molecular Formula: C₂₆H₂₃ClN₄O₂
• Molecular Weight: 458.947

Synonyms:2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

Chemical Property of 2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

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Technology Process of 2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one

There total 4 articles about 2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-Benzyl-4-chloro-5-{N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-2H-pyridazin-3-one (96017-21-9) + benzyl chloride (100-44-7) → 2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one (96017-31-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 3h;

DOI:10.1002/jhet.5570210501

Reference yield:

2-Benzyl-4-chloro-5-hydrazino-3(2H)-pyridazinone (96017-19-5) → 2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one (96017-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / ethanol / 2 h / Heating

2: 80 percent / anhydrous K₂CO₃ / dimethylformamide / 3 h / 70 °C

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;

DOI:10.1002/jhet.5570210501

Reference yield:

ortho-anisaldehyde (135-02-4) → 2-Benzyl-5-{N-benzyl-N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-4-chloro-2H-pyridazin-3-one (96017-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / ethanol / 2 h / Heating

2: 80 percent / anhydrous K₂CO₃ / dimethylformamide / 3 h / 70 °C

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;

DOI:10.1002/jhet.5570210501

upstream raw materials:

2-Benzyl-4-chloro-5-{N'-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-hydrazino}-2H-pyridazin-3-one

benzyl chloride

2-Benzyl-4-chloro-5-hydrazino-3(2H)-pyridazinone

ortho-anisaldehyde

Downstream raw materials:

1,5-Dibenzyl-3-(2-methoxy-phenyl)-1,5-dihydro-pyrazolo[3,4-d]pyridazin-4-one

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