3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose

Base Information

Chemical Name:3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose
CAS No.:50693-03-3
Molecular Formula:C₁₇H₂₂O₅
Molecular Weight:306.359
Hs Code.:

Synonyms:3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose

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Chemical Property of 3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose

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Technology Process of 3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose

There total 6 articles about 3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 51306-24-2
3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-L-idoheptofuranose

: 50693-03-3
3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; for 48h;
DOI:10.1021/jo00320a014

Reference yield:

: 22529-61-9
(1R)-1-((3aR,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro(2,3-d)(1,3)dioxol-5-yl)ethane-1,2-diol

: 50693-03-3
3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose

Guidance literature:: Multi-step reaction with 3 steps

1: sodium bicarbonate, sodium periodate / ethanol; H₂O / 2.5 h / Ambient temperature

2: tetrahydrofuran; diethyl ether / 0.17 h / 5 °C

3: 95 percent / pyridinium chlorochromate, sodium acetate / CH₂Cl₂ / 48 h

With sodium periodate; sodium acetate; sodium hydrogencarbonate; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/jo00320a014

Reference yield:

: 18685-18-2
3-O-benzyl-1,2-5,6-O-diisopropylidene-α-D-glucofuranose

: 50693-03-3
3-O-benzyl-6,7-dideoxy-1,2-O-isopropylidene-α-D-xylo-1,5-heptofuranodiulose

Guidance literature:: Multi-step reaction with 4 steps

1: 60percent acetic acid / 16 h / Ambient temperature

2: sodium bicarbonate, sodium periodate / ethanol; H₂O / 2.5 h / Ambient temperature

3: tetrahydrofuran; diethyl ether / 0.17 h / 5 °C

4: 95 percent / pyridinium chlorochromate, sodium acetate / CH₂Cl₂ / 48 h

With sodium periodate; sodium acetate; sodium hydrogencarbonate; acetic acid; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/jo00320a014