(2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate

Base Information

• Chemical Name: (2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate
• CAS No.: 1087342-92-4
• Molecular Formula: C₃₅H₄₈O₆S₂
• Molecular Weight: 628.895

Synonyms:(2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate

Chemical Property of (2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate

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Technology Process of (2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate

There total 2 articles about (2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

C35H48O6S2 (1087342-91-3) → (2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate (1087342-92-4)

Guidance literature:

With pyridinium p-toluenesulfonate; gold(I) chloride; In tetrahydrofuran; at 50 ℃; for 22h; regioselective reaction; Inert atmosphere;

DOI:10.1021/ja807127s

Reference yield: 28.0%

C35H48O6S2 (1087342-91-3) → (2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate (1087342-92-4) + C28H42O4S2 (1192033-87-6)

Guidance literature:

With pyridinium p-toluenesulfonate; gold(I) chloride; In tetrahydrofuran; at 50 ℃; Inert atmosphere;

DOI:10.1021/ja906056v

Reference yield: 80.0%

(2S,3S,4S,6R,8S)-2-((1,3-dithian-2-yl)methyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro[5.5]undecan-4-yl benzoate (1087342-92-4) → C32H42O7 (1087342-93-5)

Guidance literature:

With water; sodium hydrogencarbonate; methyl iodide; In acetonitrile; at 50 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja807127s

upstream raw materials:

C₃₅H₄₈O₆S₂

Downstream raw materials:

C₃₂H₄₂O₇

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