tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate

Base Information

Chemical Name:tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate
CAS No.:606144-73-4
Molecular Formula:C₁₈H₂₄N₂O₃
Molecular Weight:316.4
Hs Code.:

Synonyms:tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate

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Technology Process of tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate

There total 1 articles about tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 606144-71-2
tert-butyl (1R)-2-{[(1R,2S)-3-cyano-1-methyl-2-(phenylseleno)propyl]oxy}-1-phenylethylcarbamate

: 606144-73-4
tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate

Guidance literature:: With dihydrogen peroxide; In dichloromethane; at 20 ℃;
DOI:10.1016/S0957-4166(03)00498-1

Reference yield: 95.0%

: 606144-73-4
tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate

: (2R,5R)-3-Cyanomethyl-2-methyl-5-phenyl-morpholine-4-carboxylic acid tert-butyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/S0957-4166(03)00498-1

Reference yield:

: 606144-73-4
tert-butyl (1R)-2-{[(1R,2E)-3-cyano-1-methylprop-2-enyl]oxy}-1-phenylethylcarbamate

: [(2R,3R,5R)-2-methyl-5-phenylmorpholin-3-yl]acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / sodium hydride / tetrahydrofuran / 0 - 20 °C

2: 67 percent / Me₃SiI / acetonitrile / 20 °C

With trimethylsilyl iodide; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1016/S0957-4166(03)00498-1