Technology Process of C24H21N3O5
There total 6 articles about C24H21N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C31H27N3O5;
With
lithium chloride;
In
N,N-dimethylimidazolidinone;
at 90 ℃;
for 1h;
With
hydrogenchloride;
In
N,N-dimethylimidazolidinone; water;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium periodate; potassium osmate(VI) dihydrate / 1,4-dioxane; water / 6 h / 20 °C
2.1: acetic acid / toluene / 18 h / 20 - 50 °C
3.1: potassium carbonate; sodium iodide / acetonitrile / 7 h / 20 - 90 °C
4.1: sodium hydroxide; water / ethanol / 72 h / 20 °C
4.2: 20 °C
5.1: lithium chloride / N,N-dimethylimidazolidinone / 1 h / 90 °C
5.2: 20 °C
With
potassium osmate(VI) dihydrate; sodium periodate; water; potassium carbonate; acetic acid; sodium iodide; lithium chloride; sodium hydroxide;
In
1,4-dioxane; ethanol; N,N-dimethylimidazolidinone; water; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid / toluene / 18 h / 20 - 50 °C
2.1: potassium carbonate; sodium iodide / acetonitrile / 7 h / 20 - 90 °C
3.1: sodium hydroxide; water / ethanol / 72 h / 20 °C
3.2: 20 °C
4.1: lithium chloride / N,N-dimethylimidazolidinone / 1 h / 90 °C
4.2: 20 °C
With
water; potassium carbonate; acetic acid; sodium iodide; lithium chloride; sodium hydroxide;
In
ethanol; N,N-dimethylimidazolidinone; toluene; acetonitrile;