1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane

Base Information

• Chemical Name: 1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane
• CAS No.: 128134-62-3
• Molecular Formula: C₂₀H₂₃N₃O₁₁
• Molecular Weight: 481.416
• Mol file: 128134-62-3.mol

Synonyms:1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane

Chemical Property of 1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane

There total 2 articles about 1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

1-hydroxy-11-(2',4'-dinitrophenoxy)-3,6,9-trioxaundecane (128134-69-0) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → 1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane (128134-62-3)

Guidance literature:

DOI:10.1021/jo00303a024

Reference yield:

1-(2',4'-dinitrophenoxy)-11-phenoxy-3,6,9-trioxaundecane (128134-58-7) → 1-(2',4'-dinitrophenoxy)-11-(4'-nitrophenoxy)-3,6,9-trioxaundecane (128134-63-4) + 1-(2',4'-dinitrophenoxy)-11-(2'-nitrophenoxy)-3,6,9-trioxaundecane (128134-62-3)

Guidance literature:

With Salpetersaeuretrimethylsilylester; boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 3h;

DOI:10.1021/jo00303a024

upstream raw materials:

1-(2',4'-dinitrophenoxy)-11-phenoxy-3,6,9-trioxaundecane

1-hydroxy-11-(2',4'-dinitrophenoxy)-3,6,9-trioxaundecane

ortho-nitrofluorobenzene