2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate

Base Information

Chemical Name:2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate
CAS No.:1415328-14-1
Molecular Formula:C₂₄H₂₃N₃O₄S
Molecular Weight:449.53
Hs Code.:

Synonyms:2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate

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Chemical Property of 2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate

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Technology Process of 2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate

There total 5 articles about 2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.5%

: 1415328-11-8
4-(6-(methylamino)quinoxalin-2-yl)phenol

: 6315-52-2
1,2-bis-tosyloxyethane

: 1415328-14-1
2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 10h; Reflux;
DOI:10.1016/j.ejmech.2012.08.031

Reference yield:

: C₁₅H₁₁N₃O

: 1415328-14-1
2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Reflux

2: potassium carbonate; 18-crown-6 ether / acetone / 10 h / Reflux

With sodium tetrahydroborate; 18-crown-6 ether; potassium carbonate; In methanol; acetone;
DOI:10.1016/j.ejmech.2012.08.031

Reference yield:

: 99-56-9
4-Nitrophenylene-1,2-diamine

: 1415328-14-1
2-(4-(6-(methylamino)quinoxalin-2-yl)phenoxy)ethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: dimethyl sulfoxide / 20 °C

2: hydrazine hydrate; palladium on activated charcoal / ethanol / Reflux

3: sodium methylate / methanol / 2 h / Reflux

4: sodium tetrahydroborate / methanol / 1 h / 0 °C / Reflux

5: potassium carbonate; 18-crown-6 ether / acetone / 10 h / Reflux

With sodium tetrahydroborate; 18-crown-6 ether; palladium on activated charcoal; sodium methylate; potassium carbonate; hydrazine hydrate; In methanol; ethanol; dimethyl sulfoxide; acetone;
DOI:10.1016/j.ejmech.2012.08.031