5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

Base Information

Chemical Name:5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide
CAS No.:131490-66-9
Molecular Formula:C₁₉H₁₇N₅O₂S
Molecular Weight:379.442
Hs Code.:

5-<<N'-benzoyl(thiocarbamoyl)>amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

Synonyms:5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

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Technology Process of 5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

There total 1 articles about 5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-44-7
benzyl chloride

: 131490-66-9
5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KOH powder / 1) DMF, 4 h, ice bath, 2a) RT, overnight, 2b) ice bath, 2 h

2: 88 percent / acetone / 4 h / Heating

With potassium hydroxide; In acetone;
DOI:10.1021/jo00006a033

Reference yield: 88.0%

: 131490-66-9
5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

: 131490-70-5
1-(phenylmethyl)-5-<(thiocarbamoyl)amino>-1H-imidazole-4-carboxamide

Guidance literature:: With potassium carbonate; In methanol; water; acetone; for 6h; Heating;
DOI:10.1021/jo00006a033

Reference yield:

: 131490-66-9
5-<amino>-1-(phenylmethyl)-1H-imidazole-4-carboxamide

: 14937-72-5
9-benzylguanine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / K₂CO₃ / acetone; methanol; H₂O / 6 h / Heating

2: 93 percent / 1N aq. NaOH, copper(II) acetate / 1 h / Heating

With sodium hydroxide; copper diacetate; potassium carbonate; In methanol; water; acetone;
DOI:10.1021/jo00006a033