2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Base Information

Chemical Name:2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside
CAS No.:1312312-49-4
Molecular Formula:C₂₈H₂₈ClNO₁₀
Molecular Weight:573.984
Hs Code.:

Synonyms:2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

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Chemical Property of 2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

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Technology Process of 2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

There total 3 articles about 2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 120-72-9
indole

: 1312312-40-5
2-chloro-4-iodophenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 108-24-7
acetic anhydride

: 1312312-49-4
2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: indole; 2-chloro-4-iodophenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside; With potassium carbonate; L-proline; copper(l) iodide; In dimethyl sulfoxide; at 90 ℃; Inert atmosphere;

acetic anhydride; With dmap;

Reference yield: 28.0%

: 120-72-9
indole

: 1312312-40-5
2-chloro-4-iodophenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 1312312-49-4
2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: With copper(l) iodide; potassium carbonate; L-proline; In dimethyl sulfoxide; at 90 ℃; Inert atmosphere; Sealed tube;

Reference yield:

: 116130-33-7
2-chloro-4-iodophenol

: 1312312-49-4
2-chloro-4-(indol-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / toluene / 2 h / 20 °C / Inert atmosphere; Molecular sieve

2.1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 90 °C / Inert atmosphere; Sealed tube

2.2: 2 h / Inert atmosphere; Sealed tube

With copper(l) iodide; trimethylsilyl trifluoromethanesulfonate; potassium carbonate; L-proline; In dimethyl sulfoxide; toluene;
DOI:10.1021/jm300192x