2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole

Base Information

• Chemical Name: 2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole
• CAS No.: 1029931-24-5
• Molecular Formula: C₄₉H₅₆N₂O₆SSi₂
• Molecular Weight: 857.23

Synonyms:2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole

Chemical Property of 2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole

Chemical Property:

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Technology Process of 2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole

There total 1 articles about 2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribofuranose (1029931-23-4) + 2-(N-methylbenzamido)thiazole (118215-02-4) → 2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole (1029931-24-5)

Guidance literature:

2-(N-methylbenzamido)thiazole; With lithium diisopropylammonium; In tetrahydrofuran; at -78 ℃; for 0.5h;

3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribofuranose; In tetrahydrofuran; at -78 ℃; for 1h; Further stages.;

DOI:10.1016/j.bmc.2007.12.043

Reference yield: 64.0%

2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribitol-1-yl)thiazole (1029931-24-5) → 2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribofuranosyl)thiazole (1029931-25-6)

Guidance literature:

With tributylphosphine; diamide; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1016/j.bmc.2007.12.043

upstream raw materials:

3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribofuranose

2-(N-methylbenzamido)thiazole

Downstream raw materials:

2-(N-methylbenzamido)-5-(3,5-di-O-tert-butyldiphenylsilyl-2-O,4-C-methylene-D-ribofuranosyl)thiazole

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