1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione
CAS No.:99328-77-5
Molecular Formula:C₄₁H₅₂N₂O₁₃
Molecular Weight:780.869
Hs Code.:

1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

Synonyms:1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

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Chemical Property of 1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

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Technology Process of 1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

There total 1 articles about 1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60043-43-8
<(2-methoxyethoxy)methyl>triethylammonium chloride

: 51600-12-5
5'-O-monomethoxytrityluridine

: 99328-77-5
1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

Guidance literature:: In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/jo00356a033

Reference yield:

: 99328-77-5
1-{(2R,3R,4R,5R)-3,4-Bis-(2-methoxy-ethoxymethoxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

: 58-96-8
uridine

Guidance literature:: Multi-step reaction with 3 steps

1: 80percent aq. AcOH / 6 h / Ambient temperature

2: 10 percent / triphenylmethyl fluoroborate (TrBF) / acetonitrile; H₂O / 2 h / Ambient temperature

3: 94 percent / conc. ammonia, pyridine / 5 h / 50 °C

With pyridine; ammonium hydroxide; trityl tetrafluoroborate; acetic acid; In water; acetonitrile;
DOI:10.1021/jo00356a033