(2R, 3R, 11bS)-(+)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzoquinolizine-2-acetamide

Base Information

• Chemical Name: (2R, 3R, 11bS)-(+)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzo
• Molecular Formula: C₃₆H₄₃N₃O₄
• Molecular Weight: 581.755

Synonyms:(2R, 3R, 11bS)-(+)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzoquinolizine-2-acetamide

Chemical Property of (2R, 3R, 11bS)-(+)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzo

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There total 2 articles about (2R, 3R, 11bS)-(+)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzoquinolizine-2-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

tryptamine (61-54-1) + (+/-)-8-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine-2β-acetic acid (61194-41-0,65942-18-9) → (+/-)-8-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzoquinolizine-2β-acetamide (65891-86-3,69461-01-4)

Guidance literature:

With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; at 30 ℃; for 6h;

DOI:10.1248/cpb.33.1946

Reference yield: 92.0%

tryptamine (61-54-1) + (2R,3R,11bS)-(-)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2H-benzoquinolizine-2-acetic acid (61194-41-0,65942-18-9) → (2R, 3R, 11bS)-(+)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzoquinolizine-2-acetamide (69461-01-4)

Guidance literature:

With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; at 28 ℃; for 6h;

DOI:10.1248/cpb.33.1946

Reference yield: 82.0%

(2R, 3R, 11bS)-(+)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-N-<2-(indol-3-yl)ethyl>-9,10-dimethoxy-2H-benzoquinolizine-2-acetamide (69461-01-4) → (2R, 3R, 11bS)-(+)-8-benzyloxy-2-<(4,9-dihydro-3H-pyrido<3,4b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine (69437-62-3)

Guidance literature:

With trichlorophosphate; In toluene; for 2.5h; Heating;

DOI:10.1248/cpb.33.1946

upstream raw materials:

tryptamine

(+/-)-8-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine-2β-acetic acid

(2R,3R,11bS)-(-)-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2H-benzoquinolizine-2-acetic acid

Downstream raw materials:

(+/-)-8-benzyloxy-2β-<(4,9-dihydro-3H-pyrido<3,4b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine

(2R, 3R, 11bS)-(+)-8-benzyloxy-2-<(4,9-dihydro-3H-pyrido<3,4b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine

alangimarckine

<2S-<2α(R^*),3β,11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine

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