N¹,N¹,N³,N³,N⁵,N⁵-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine

Base Information

• Chemical Name: N¹,N¹,N³,N³,N⁵,N⁵-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine
• CAS No.: 165820-83-7
• Molecular Formula: C₆₆H₈₁N₃
• Molecular Weight: 916.389
• Mol file: 165820-83-7.mol

Synonyms:N¹,N¹,N³,N³,N⁵,N⁵-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine

Chemical Property of N¹,N¹,N³,N³,N⁵,N⁵-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N¹,N¹,N³,N³,N⁵,N⁵-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine

There total 4 articles about N¹,N¹,N³,N³,N⁵,N⁵-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,3,5-trisbromobenzene (626-39-1) + bis(4-tert-butylphenyl)amine (4627-22-9) → N1,N1,N3,N3,N5,N5-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine (165820-83-7)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In toluene; at 90 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.202012891

Reference yield: 20.0%

1-tert-butyl-4-iodobenzene (35779-04-5) + N1,N3,N5-tris(4-tert-butylphenyl)benzene-1,3,5-triamine (165820-78-0) → N1,N1,N3,N3,N5,N5-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine (165820-83-7)

Guidance literature:

With copper; at 180 ℃; for 24h;

DOI:10.1016/0040-4039(95)00094-S

Reference yield:

1,3,5-Triiodobenzene (626-44-8) + bis(4-tert-butylphenyl)amine (4627-22-9) → N1,N1,N3,N3,N5,N5-hexakis(4-(tert-butyl)phenyl)benzene-1,3,5-triamine (165820-83-7)

Guidance literature:

With pyridine; copper(l) iodide; n-butyllithium; Yield given. Multistep reaction;

DOI:10.1246/cl.1995.1011

upstream raw materials:

1-tert-butyl-4-iodobenzene

N¹,N³,N⁵-tris(4-tert-butylphenyl)benzene-1,3,5-triamine

1,3,5-Triiodobenzene

bis(4-tert-butylphenyl)amine