2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole

Base Information

• Chemical Name: 2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole
• CAS No.: 1304568-31-7
• Molecular Formula: C₁₉H₁₇N₅S
• Molecular Weight: 347.443

Synonyms:2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole

Chemical Property of 2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole

Chemical Property:

Purity/Quality:

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Technology Process of 2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole

There total 2 articles about 2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

acetonitrile (75-05-8,26809-02-9) + 2-(4-methylbenzylidene)-1-(5-(4-methylphenyl)-1,3,4-thiadiazol-2-yl)hydrazine → 2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole (1304568-31-7) + 3,6-bis(4-methylphenyl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole (193744-07-9)

Guidance literature:

With lithium perchlorate; at 20 ℃; Electrochemical reaction;

DOI:10.1016/j.tet.2011.02.084

Reference yield:

N,N-bis[(4-methylphenyl)methylidene]carbothioic dihydrazide → 2-(5-methyl-3-(4-methylphenyl)-1H-[1,2,4]triazol-1-yl)-5-(4-methylphenyl)-1,3,4-thiadiazole (1304568-31-7) + 3,6-bis(4-methylphenyl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole (193744-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: iron(III) chloride / ethanol / 0.5 h / Reflux

2: lithium perchlorate / 20 °C / Electrochemical reaction

With iron(III) chloride; lithium perchlorate; In ethanol;

DOI:10.1016/j.tet.2011.02.084

upstream raw materials:

acetonitrile

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