2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Base Information

Chemical Name:2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate
CAS No.:290297-88-0
Molecular Formula:C₂₅H₃₀N₄O₄
Molecular Weight:450.538
Hs Code.:

Synonyms:2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

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Chemical Property of 2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

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Technology Process of 2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

There total 7 articles about 2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 290297-90-4
1,3-dimethyl-2-(4-formylphenyl)-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

: 290297-88-0
2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Guidance literature:: In methanol; chloroform; at 60 ℃; for 18h;
DOI:10.1021/ol0060329

Reference yield:

: 15781-73-4
di(2,4,6-trichlorophenyl)-2-phenylmalonate

: 290297-88-0
2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / methoxybenzene / 0.05 h / Heating

2: 88 percent / Lewatit S 100 / acetonitrile / 1 h / Heating

3: 52 percent / methanol; CHCl₃ / 18 h / 60 °C

With Lewatit S 100; In methanol; chloroform; methoxybenzene; acetonitrile; 1: cyclocondensation / 2: Elimination / 3: cyclocondensation;
DOI:10.1021/ol0060329

Reference yield:

: 623-27-8
terephthalaldehyde,

: 290297-88-0
2-[4-(1,3-dihydroxy-4,4,5,5-tetramethyl-1,3-imidazolidin-2-yl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 16 percent / conc. H₂SO₄ / ethanol / 12 h / 20 °C

2.1: 69 percent / sulphur / ethanol / 4 h / 110 °C

3.1: diethyl ether / 70 h / 20 °C

3.2: 83 percent / ethanol / 7.5 h

4.1: 69 percent / methoxybenzene / 0.05 h / Heating

5.1: 88 percent / Lewatit S 100 / acetonitrile / 1 h / Heating

6.1: 52 percent / methanol; CHCl₃ / 18 h / 60 °C

With Lewatit S 100; sulfuric acid; sulfur; In methanol; diethyl ether; ethanol; chloroform; methoxybenzene; acetonitrile; 1.1: acetalization / 2.1: Wilgerodt-Kindler reaction / 3.1: Methylation / 3.2: Substitution / 4.1: cyclocondensation / 5.1: Elimination / 6.1: cyclocondensation;
DOI:10.1021/ol0060329