(3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone

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Chemical Name:(3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone
CAS No.:74158-41-1
Molecular Formula:C₂₀H₂₇N₃O₆
Molecular Weight:405.451
Hs Code.:

Synonyms:(3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone

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Chemical Property of (3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone

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Technology Process of (3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone

There total 6 articles about (3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 74863-00-6
(S)-2-(2-Oxo-propionylamino)-propionic acid (S)-1-((S)-1-carbamoyl-2-phenyl-ethylcarbamoyl)-2-methyl-propyl ester

: 74158-41-1
(3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone

Guidance literature:: With hydrogen fluoride; at 0 ℃; for 1h;
DOI:10.1016/S0040-4039(00)71467-5

Reference yield:

: 65864-22-4
(S)-2-amino-3-phenylpropionamide hydrochloride

: 74158-41-1
(3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / 1-ethyl-3-(3'-dimethylaminopropyl)carbodiimide

3: 1-ethyl-3-(3'-dimethylaminopropyl)carbodiimide

4: H₂O, 1M HCl / acetic acid

5: 74 percent / HF / 1 h / 0 °C

With hydrogenchloride; hydrogen fluoride; water; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In acetic acid;
DOI:10.1016/S0040-4039(00)71467-5

Reference yield:

: 74862-99-0
(S)-2-Amino-propionic acid (S)-1-((S)-1-carbamoyl-2-phenyl-ethylcarbamoyl)-2-methyl-propyl ester

: 74158-41-1
(3S,9S,12S)-9-Benzyl-6-hydroxy-12-isopropyl-3,6-dimethyl-1-oxa-4,7,10-triaza-cyclododecane-2,5,8,11-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-3-(3'-dimethylaminopropyl)carbodiimide

2: H₂O, 1M HCl / acetic acid

3: 74 percent / HF / 1 h / 0 °C

With hydrogenchloride; hydrogen fluoride; water; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In acetic acid;
DOI:10.1016/S0040-4039(00)71467-5