N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

Base Information

Chemical Name:N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide
CAS No.:866482-46-4
Molecular Formula:C₄₀H₅₇N₃O₈
Molecular Weight:707.908
Hs Code.:

<i>N</i>-(5-amino-2,4-dimethoxy-phenyl)-<i>N</i>'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

Synonyms:N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

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Chemical Property of N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

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Technology Process of N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

There total 7 articles about N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 866482-45-3
N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid

: 1129-15-3
4,6-dimethoxy-benzene-1,3-diamine

: 866482-46-4
N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1039/b508773b

Reference yield:

: 89-39-4
1,4-dimethoxy-2-nitrobenzene

: 866482-46-4
N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / hydrogen / Pd/C / tetrahydrofuran / 8 h / 20 °C / 760 Torr

2: 1.84 g / triethylamine / CHCl₃ / 10 h / 20 °C

3: 96 percent / potassium hydroxide / H₂O; methanol / 3 h / Heating

4: 67 percent / N-ethyl-N'-(3-dimethyl-aminopropyl) carbodiimide / CH₂Cl₂ / 6 h / 20 °C

With potassium hydroxide; hydrogen; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; chloroform; water;
DOI:10.1039/b508773b

Reference yield:

: 866482-43-1
5-chlorocarbonyl-2,4-bis-octyloxy-benzoic acid methyl ester

: 866482-46-4
N-(5-amino-2,4-dimethoxy-phenyl)-N'-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.84 g / triethylamine / CHCl₃ / 10 h / 20 °C

2: 96 percent / potassium hydroxide / H₂O; methanol / 3 h / Heating

3: 67 percent / N-ethyl-N'-(3-dimethyl-aminopropyl) carbodiimide / CH₂Cl₂ / 6 h / 20 °C

With potassium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In methanol; dichloromethane; chloroform; water;
DOI:10.1039/b508773b