(S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

Base Information

Chemical Name:(S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate
CAS No.:1403666-33-0
Molecular Formula:C₂₆H₃₂BrNO₄S
Molecular Weight:534.514
Hs Code.:

Synonyms:(S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

Suppliers and Price of (S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

There total 9 articles about (S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1403666-31-8
(S)-2-(7-bromo-2-chloro-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

: 100-51-6,185532-71-2
benzyl alcohol

: 1403666-33-0
(S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

Guidance literature:: benzyl alcohol; With sodium hydride; at 20 ℃; for 0.5h;

(S)-2-(7-bromo-2-chloro-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate; at 60 ℃; for 0.75h;

Reference yield:

: 1403666-50-1
(S)-2-(2-bromo-6-methyl-4-nitrophenyl)-2-hydroxyethyl pivalate

: 1403666-33-0
(S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

Guidance literature:: Multi-step reaction with 5 steps

1.1: perchloric acid / 3.08 h / 0 - 20 °C

2.1: hydrogen / platinum on activated charcoal / ethyl acetate; ethanol / 5 h / 20 °C

3.1: acetic acid / tetrahydrofuran / 0.5 h / 0 °C

4.1: tert.-butylnitrite; copper dichloride / acetonitrile / 20 °C

5.1: sodium hydride / 0.5 h / 20 °C

5.2: 0.75 h / 60 °C

With tert.-butylnitrite; perchloric acid; hydrogen; sodium hydride; acetic acid; copper dichloride; platinum on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate; acetonitrile;

Reference yield:

: 1403666-51-2
(S)-2-(2-bromo-6-methyl-4-nitrophenyl)-2-tert-butoxyethyl pivalate

: 1403666-33-0
(S)-2-(2-(benzyloxy)-7-bromo-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyethyl pivalate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / platinum on activated charcoal / ethyl acetate; ethanol / 5 h / 20 °C

2.1: acetic acid / tetrahydrofuran / 0.5 h / 0 °C

3.1: tert.-butylnitrite; copper dichloride / acetonitrile / 20 °C

4.1: sodium hydride / 0.5 h / 20 °C

4.2: 0.75 h / 60 °C

With tert.-butylnitrite; hydrogen; sodium hydride; acetic acid; copper dichloride; platinum on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate; acetonitrile;