Technology Process of C42H62N4O6
There total 7 articles about C42H62N4O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
for 20h;
under 30400 Torr;
DOI:10.1016/j.tet.2006.09.073
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / sulfuric acid; nitric acid / 2 h / 20 °C
2: 85 percent / sodium hydroxide / tetrahydrofuran; methanol; H2O / 12 h / 20 °C
3: oxalyl chloride / dimethylformamide; benzene / 1 h / 20 °C
4: 90 percent / triethylamine / CH2Cl2 / 2 h / 20 °C
5: 95 percent / hydrogen / Pd-C / tetrahydrofuran / 20 h / 30400 Torr
With
sodium hydroxide; oxalyl dichloride; sulfuric acid; hydrogen; nitric acid; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tet.2006.09.073
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / triethylamine / CH2Cl2 / 2 h / 20 °C
2: 95 percent / hydrogen / Pd-C / tetrahydrofuran / 20 h / 30400 Torr
With
hydrogen; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2006.09.073