3,4-dimethoxybenzenecarbodithioic acid benzyl ester

Base Information

• Chemical Name: 3,4-dimethoxybenzenecarbodithioic acid benzyl ester
• CAS No.: 155855-94-0
• Molecular Formula: C₁₆H₁₆O₂S₂
• Molecular Weight: 304.434
• Mol file: 155855-94-0.mol

Synonyms:3,4-dimethoxybenzenecarbodithioic acid benzyl ester

Chemical Property of 3,4-dimethoxybenzenecarbodithioic acid benzyl ester

Chemical Property:

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Technology Process of 3,4-dimethoxybenzenecarbodithioic acid benzyl ester

There total 1 articles about 3,4-dimethoxybenzenecarbodithioic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Veratric acid (93-07-2) + benzyl alcohol (100-51-6,185532-71-2) → 3,4-dimethoxybenzenecarbodithioic acid benzyl ester (155855-94-0)

Guidance literature:

With Lawessons reagent; In toluene; at 120 ℃; for 48h;

DOI:10.1021/ja0756321

Reference yield:

piperonyl 4-fluorodithiobenzoate + 3,4-dimethoxybenzenecarbodithioic acid benzyl ester (155855-94-0) → piperonyl 3,4-dimethoxydithiobenzoate + benzyl 4-fluorodithiobenzoate (305378-88-5)

Guidance literature:

2,2'-azobis(isobutyronitrile); In toluene; at 120 ℃; for 5h;

DOI:10.1021/ja0756321

upstream raw materials:

Veratric acid

benzyl alcohol

Downstream raw materials:

benzyl 4-fluorodithiobenzoate