1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

Base Information

Chemical Name:1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene
CAS No.:59830-46-5
Molecular Formula:C₂₇H₃₅F₃O₃S
Molecular Weight:496.634
Hs Code.:

Synonyms:1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

Suppliers and Price of 1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

There total 6 articles about 1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.5%

: 59830-41-0
1-(p-trifluoromethylphenylsulfonyl)-2-methyl-4-hydroxy-but-2-ene

: 55732-70-2
5-(2,6,6-trimethyl-cyclohex-1-enyl)-3-methyl-1-chloro-penta-2,4-diene

: 59830-46-5
1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

Guidance literature:: With hydrogenchloride; n-butyllithium; In tetrahydrofuran;

Reference yield:

: 24529-80-4
(E)-1-O-acetyl-4-chloro-3-methyl-2-buten-1-ol

: 59830-46-5
1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide

2: LiAlH₄ / tetrahydrofuran

3: nBuLi / tetrahydrofuran

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00882a017

Reference yield:

: 59057-30-6
(1E)-1-(2,6,6-trimethylcyclohex-1-enyl)-3-methyl-1,4-pentadien-3-ol

: 59830-46-5
1-hydroxy-3,7-dimethyl-4-(p-trifluoromethylphenylsulfonyl)-9-(2,6,6-trimethylcyclohexen-1-yl)-nona-2,6,8-triene

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / diethyl ether

2: nBuLi / tetrahydrofuran

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00882a017