allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester
CAS No.:884864-65-7
Molecular Formula:C₃₃H₄₀N₂O₆
Molecular Weight:560.69
Hs Code.:

allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid <i>tert</i>-butyl ester

Synonyms:allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester

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Chemical Property of allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester

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Technology Process of allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester

There total 8 articles about allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-{3-[(allyl-tert-butoxycarbonyl-amino)-methyl]-furan-2-yl}-4-benzyloxy-6-hydroxy-benzoic acid

: 34825-70-2
hex-5-en-1-amine

: 884864-65-7
allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester

Guidance literature:: DOI:10.1016/j.tetlet.2006.01.117

Reference yield:

: 83-30-7
acide 2,4,6-trihydroxybenzoique

: 884864-65-7
allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: trifluoroacetic acid; trifluoroacetic anhydride

2: pyridine / CH₂Cl₂

3: Pd(Ph₃P)2Cl₂ / dimethylformamide / 1 h / 60 °C

4: NaBH(OAc)3; 4 Angstroem molecular sieves / CH₂Cl₂ / 2 h / 20 °C

5: CH₂Cl₂ / 3 h

6: KOH / dimethylsulfoxide / 1 h / 65 °C

With pyridine; potassium hydroxide; 4 A molecular sieve; sodium tris(acetoxy)borohydride; trifluoroacetic acid; trifluoroacetic anhydride; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; 2: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2006.01.117

Reference yield:

: 137571-73-4
5,7-dihydroxy-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one

: 884864-65-7
allyl-[2-(5-benzyloxy-2-hex-5-enylcarbamoyl-3-hydroxy-phenyl)-furan-3-ylmethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / CH₂Cl₂

2: Pd(Ph₃P)2Cl₂ / dimethylformamide / 1 h / 60 °C

3: NaBH(OAc)3; 4 Angstroem molecular sieves / CH₂Cl₂ / 2 h / 20 °C

4: CH₂Cl₂ / 3 h

5: KOH / dimethylsulfoxide / 1 h / 65 °C

With pyridine; potassium hydroxide; 4 A molecular sieve; sodium tris(acetoxy)borohydride; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; 1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2006.01.117