N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester

Base Information

Chemical Name:N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester
CAS No.:158975-64-5
Molecular Formula:C₃₄H₄₀N₂O₉
Molecular Weight:620.7
Hs Code.:

Synonyms:N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester

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Chemical Property of N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester

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Technology Process of N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester

There total 2 articles about N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 158975-62-3
methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

: 158975-64-5
N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(94)84216-7

Reference yield:

: 158975-58-7
methyl 3,4,6-tri-O-benzyl-2-C-(N-tert-butoxycarbonylmethylcarbamoyl)-2-deoxy-β-D-glucopyranoside

: 158975-64-5
N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂ / 1.5 h / Ambient temperature

2: 67 percent / Et₃N, 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/0008-6215(94)84216-7