3,5-bis(trifluoromethylsulfonyl)benzoic Acid

Base Information

Chemical Name:3,5-bis(trifluoromethylsulfonyl)benzoic Acid
CAS No.:102117-41-9
Molecular Formula:C₉H₄F₆O₆S₂
Molecular Weight:386.25
Hs Code.:
European Community (EC) Number:853-388-6

Synonyms:3,5-bis(trifluoromethylsulfonyl)benzoic Acid;3,5-Bis((trifluoromethyl)sulfonyl)benzoic acid;102117-41-9;3,5-DITRIFLUOROMETHANESULFONYLBENZOIC ACID;starbld0003380;SCHEMBL18513400;QSDVQFLPFNXAOZ-UHFFFAOYSA-N;AKOS003621160;CS-0243584;EN300-26601029;Z56850657

Suppliers and Price of 3,5-bis(trifluoromethylsulfonyl)benzoic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3,5-bis(trifluoromethylsulfonyl)benzoic Acid

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:12
Rotatable Bond Count:3
Exact Mass:385.93534916
Heavy Atom Count:23
Complexity:613

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=C(C=C(C=C1S(=O)(=O)C(F)(F)F)S(=O)(=O)C(F)(F)F)C(=O)O

Technology Process of 3,5-bis(trifluoromethylsulfonyl)benzoic Acid

There total 3 articles about 3,5-bis(trifluoromethylsulfonyl)benzoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 102117-40-8
3,5-bis(trifluoromethylthio)benzoic acid

: 102117-41-9
3,5-bis(trifluoromethylsulfonyl)benzoic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In acetic acid; 1.)20-25 deg C, 1 h 2.)45-50 deg C, 4 h;

Reference yield:

: 21829-31-2
3,5-bis-chlorosulfonyl-benzoic acid

: 102117-41-9
3,5-bis(trifluoromethylsulfonyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / Zn dust/conc. aq. HCl / benzene; dioxane / 1.5 h / Heating

2: 89 percent / NH₃(l) / 0.67 h / Irradiation

3: 88 percent / CrO₃/H₂SO₄ / acetic acid / 1.)20-25 deg C, 1 h 2.)45-50 deg C, 4 h

With chromium(VI) oxide; hydrogenchloride; sulfuric acid; ammonia; zinc; In 1,4-dioxane; acetic acid; benzene;

Reference yield:

: 102117-39-5
3,5-dimercaptobenzoic acid

: 102117-41-9
3,5-bis(trifluoromethylsulfonyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NH₃(l) / 0.67 h / Irradiation

2: 88 percent / CrO₃/H₂SO₄ / acetic acid / 1.)20-25 deg C, 1 h 2.)45-50 deg C, 4 h

With chromium(VI) oxide; sulfuric acid; ammonia; In acetic acid;