1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

Base Information

Chemical Name:1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone
CAS No.:1616469-66-9
Molecular Formula:C₁₉H₁₇NO₂
Molecular Weight:291.349
Hs Code.:

Synonyms:1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

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Chemical Property of 1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

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Technology Process of 1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

There total 6 articles about 1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1616469-49-8
C₁₉H₁₉NO₂

: 1616469-66-9
1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

: 1616469-84-1
(E)-N-(4-(4-methylbenzylidene)chroman-5-yl)acetamide

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In acetonitrile; at 120 ℃; for 6h; Solvent; Glovebox;
DOI:10.1039/c4cc02398f

Reference yield: 60.0%

: 1616469-49-8
C₁₉H₁₉NO₂

: 1616469-66-9
1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

Guidance literature:: With tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; oxygen; copper(II) acetate monohydrate; In acetone; at 20 ℃; for 16h;
DOI:10.1039/c4cc02947j

Reference yield:

: 554-84-7
meta-nitrophenol

: 1616469-66-9
1-(4-(p-tolyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

: 1616469-84-1
(E)-N-(4-(4-methylbenzylidene)chroman-5-yl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

3: zinc; acetic acid / dichloromethane / 0 °C

4: triethylamine; pyridine / dichloromethane / 0 °C

5: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; silver hexafluoroantimonate / acetonitrile / 6 h / 120 °C / Glovebox

With pyridine; bis-triphenylphosphine-palladium(II) chloride; silver hexafluoroantimonate; copper(l) iodide; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; di-isopropyl azodicarboxylate; copper(II) acetate monohydrate; acetic acid; triethylamine; triphenylphosphine; zinc; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1039/c4cc02398f