Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester

Base Information

Chemical Name:Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester
CAS No.:303176-76-3
Molecular Formula:C₃₁H₃₄ClNO₅
Molecular Weight:536.068
Hs Code.:

Synonyms:Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester

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Chemical Property of Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester

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Technology Process of Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester

There total 1 articles about Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33842-02-3,529510-96-1
dichloromethylenedimethyliminium chloride

: 221371-25-1
(1R,2R,3R,4R)-3,4-di-O-benzyl-5-(benzyloxymethyl)cyclohex-5-ene-1,2,3,4-tetraol

: 303176-76-3
Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester

Guidance literature:: With triethylamine; In dichloromethane; Heating;
DOI:10.1016/S0040-4039(00)01150-3

Reference yield: 98.0%

: 110-91-8,99108-56-2
morpholine

: 303176-76-3
Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester

: Dimethyl-carbamic acid (5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-cyclohexa-1,3-dienyl ester

: Dimethyl-carbamic acid (1R,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-morpholin-4-yl-cyclohex-3-enyl ester

Guidance literature:: With triethylamine; trimethylolpropane phosphite; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In acetonitrile; at 50 - 55 ℃; for 24h;
DOI:10.1016/S0040-4039(00)01150-3

Reference yield: 94.0%

: 111-86-4
n-Octylamine

: 303176-76-3
Dimethyl-carbamic acid (1S,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-chloro-cyclohex-3-enyl ester

: Dimethyl-carbamic acid (5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-cyclohexa-1,3-dienyl ester

: Dimethyl-carbamic acid (1R,2S,5R,6S)-5,6-bis-benzyloxy-4-benzyloxymethyl-2-octylamino-cyclohex-3-enyl ester

Guidance literature:: With triethylamine; trimethylolpropane phosphite; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In acetonitrile; at 50 - 55 ℃; for 24h;
DOI:10.1016/S0040-4039(00)01150-3