[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]ClO₄

Base Information

• Chemical Name: [Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]ClO₄
• CAS No.: 84190-53-4
• Molecular Formula: C₅₅H₄₅As₂O₃PRh*ClO₄
• Molecular Weight: 1137.13

Synonyms:[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]ClO₄

Chemical Property of [Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]ClO₄

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Technology Process of [Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]ClO₄

There total 2 articles about [Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OAs(C₆H₅)3)2(P(C₆H₅)3)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

[Rh((CHCHC2H4)2)(OAs(C6H5)3)2](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OAs(C6H5)3)2]ClO4 (84190-91-0) → [Rh(CO)(OAs(C6H5)3)2(P(C6H5)3)](1+)*ClO4(1-)=[Rh(CO)(OAs(C6H5)3)2(P(C6H5)3)]ClO4 (84190-53-4)

Guidance literature:

With PPh₃; CO; In dichloromethane; CO bubbled through complex soln. for 15 min, stoich. amt. of PPh3/CH2Cl2 added, stirred for 30 min at room temp.; concd. (vac.), crystd. (ether), filtered off, washed with ether, air-dried; elem. anal.;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

[Rh(CO)2(OAs(C6H5)3)2](1+)*ClO4(1-)=[Rh(CO)2(OAs(C6H5)3)2]ClO4 (84214-27-7) → [Rh(CO)(OAs(C6H5)3)2(P(C6H5)3)](1+)*ClO4(1-)=[Rh(CO)(OAs(C6H5)3)2(P(C6H5)3)]ClO4 (84190-53-4)

Guidance literature:

With PPh₃; In dichloromethane; stoich. amt. of ligand added to complex soln. at room temp.;

DOI:10.1016/S0022-328X(00)85856-8

upstream raw materials:

[Rh(CO)2(OAs(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)2(OAs(C₆H₅)3)2]ClO₄

[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)2]ClO₄

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