3-(2,2,2-triphenylethoxy)-3-chlorodiazirine

Base Information

• Chemical Name: 3-(2,2,2-triphenylethoxy)-3-chlorodiazirine
• CAS No.: 913723-48-5
• Molecular Formula: C₂₁H₁₇ClN₂O
• Molecular Weight: 348.832
• Mol file: 913723-48-5.mol

Synonyms:3-(2,2,2-triphenylethoxy)-3-chlorodiazirine

Chemical Property of 3-(2,2,2-triphenylethoxy)-3-chlorodiazirine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2,2,2-triphenylethoxy)-3-chlorodiazirine

There total 2 articles about 3-(2,2,2-triphenylethoxy)-3-chlorodiazirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenyl isouronium methanesulfonate → 3-(2,2,2-triphenylethoxy)-3-chlorodiazirine (913723-48-5)

Guidance literature:

With lithium chloride; In dimethyl sulfoxide; pentane;

DOI:10.1021/ol061863l

Reference yield:

2,2,2-triphenylethanol (896-32-2) → 3-(2,2,2-triphenylethoxy)-3-chlorodiazirine (913723-48-5)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 24 h / 20 °C

2: LiCl / dimethylsulfoxide; pentane

With lithium chloride; In tetrahydrofuran; dimethyl sulfoxide; pentane;

DOI:10.1021/ol061863l

Reference yield: 91.0%

3-(2,2,2-triphenylethoxy)-3-chlorodiazirine (913723-48-5) → C21H18Cl2O + Triphenylethylene (58-72-0)

Guidance literature:

In chloroform-d1; for 2h; Title compound not separated from byproducts; Photolysis;

DOI:10.1021/ol061863l

upstream raw materials:

2,2,2-triphenylethanol

Downstream raw materials:

Triphenylethylene

2,2,2-triphenylethanol