Technology Process of C56H74O25
There total 31 articles about C56H74O25 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / hex-1-ene, ethyldiisopropylamine / CH2Cl2 / 36 h / 23 °C
2: 83 percent / H2, AcOH / Pd-C / ethanol / 24 h / 23 °C / 10343 Torr
3: 1.) Ag2CO3, 4 Angstroem molecular sieves, 2.) AgClO4 / 1) CH2Cl2, 23 deg C, 1 h; 2) CH2Cl2, 23 deg C, 12 h
With
1-hexene; 4 A molecular sieve; hydrogen; silver perchlorate; acetic acid; N-ethyl-N,N-diisopropylamine; silver carbonate;
palladium on activated charcoal;
In
ethanol; dichloromethane;
DOI:10.1021/jo962300y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / hex-1-ene, ethyldiisopropylamine / CH2Cl2 / 36 h / 23 °C
2: 83 percent / H2, AcOH / Pd-C / ethanol / 24 h / 23 °C / 10343 Torr
3: 1.) Ag2CO3, 4 Angstroem molecular sieves, 2.) AgClO4 / 1) CH2Cl2, 23 deg C, 1 h; 2) CH2Cl2, 23 deg C, 12 h
With
1-hexene; 4 A molecular sieve; hydrogen; silver perchlorate; acetic acid; N-ethyl-N,N-diisopropylamine; silver carbonate;
palladium on activated charcoal;
In
ethanol; dichloromethane;
DOI:10.1021/jo962300y
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bromine / CH2Cl2 / 0.08 h / 0 - 23 °C
2: 80 percent / hex-1-ene, ethyldiisopropylamine / CH2Cl2 / 36 h / 23 °C
3: 83 percent / H2, AcOH / Pd-C / ethanol / 24 h / 23 °C / 10343 Torr
4: 1.) Ag2CO3, 4 Angstroem molecular sieves, 2.) AgClO4 / 1) CH2Cl2, 23 deg C, 1 h; 2) CH2Cl2, 23 deg C, 12 h
With
1-hexene; 4 A molecular sieve; hydrogen; bromine; silver perchlorate; acetic acid; N-ethyl-N,N-diisopropylamine; silver carbonate;
palladium on activated charcoal;
In
ethanol; dichloromethane;
DOI:10.1021/jo962300y