C₂₄H₃₃NO₅Si

Base Information

Chemical Name:C₂₄H₃₃NO₅Si
CAS No.:1333145-71-3
Molecular Formula:C₂₄H₃₃NO₅Si
Molecular Weight:443.615
Hs Code.:

C<sub>24</sub>H<sub>33</sub>NO<sub>5</sub>Si

Synonyms:C₂₄H₃₃NO₅Si

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Chemical Property of C₂₄H₃₃NO₅Si

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Technology Process of C₂₄H₃₃NO₅Si

There total 1 articles about C₂₄H₃₃NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 26348-61-8,104055-46-1
L-serine ethyl ester hydrochloride

: 125941-75-5
(S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoic acid

: 1333145-71-3
C₂₄H₃₃NO₅Si

Guidance literature:: (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;

L-serine ethyl ester hydrochloride; With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1055/s-0030-1260806

Reference yield: 59.0%

: 1333145-71-3
C₂₄H₃₃NO₅Si

: 1333145-72-4
C₂₄H₃₁NO₄Si

Guidance literature:: C₂₄H₃₃NO₅Si; With diethylamino-sulfur trifluoride; In tetrahydrofuran; at -78 ℃; for 1.5h;

With potassium carbonate; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1055/s-0030-1260806

Reference yield:

: 1333145-71-3
C₂₄H₃₃NO₅Si

: C₃₅H₅₃N₅O₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: diethylamino-sulfur trifluoride / tetrahydrofuran / 1.5 h / -78 °C

1.2: -78 - 20 °C

2.1: hexamethylenetetramine; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper(ll) bromide / dichloromethane / 0 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 - 20 °C

4.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran

6.1: dimethylsulfide borane complex; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 0 °C

7.1: dichloromethane / 0 - 20 °C

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

8.2: 0 - 20 °C

9.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 0 - 20 °C

10.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

10.2: 0 - 20 °C

11.1: tetrahydrofuran; dichloromethane / 0 - 20 °C

12.1: 1-hydroxy-7-aza-benzotriazole; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate

12.2: 0 - 20 °C

13.1: water; lithium hydroxide / tetrahydrofuran / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; diethylamino-sulfur trifluoride; dimethylsulfide borane complex; hexamethylenetetramine; tetrabutyl ammonium fluoride; water; sodium hydride; benzotriazol-1-ol; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; copper(ll) bromide; lithium hydroxide; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; 4.1: Dess-Martin oxidation;
DOI:10.1055/s-0030-1260806