Boc-Gln-Pro-OBzl*HCl

Base Information

Chemical Name:Boc-Gln-Pro-OBzl*HCl
CAS No.:40162-66-1
Molecular Formula:C₂₂H₃₁N₃O₆
Molecular Weight:433.505
Hs Code.:

Synonyms:Boc-Gln-Pro-OBzl*HCl

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Chemical Property of Boc-Gln-Pro-OBzl*HCl

Chemical Property:

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Technology Process of Boc-Gln-Pro-OBzl*HCl

There total 1 articles about Boc-Gln-Pro-OBzl*HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (4-hydroxyphenyl)(methyl)(benzyl)sulfonium chloride

: 2419-99-0
(S)-1-((S)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyryl)-pyrrolidine-2-carboxylic acid

: 40162-66-1
Boc-Gln-Pro-OBzl*HCl

Guidance literature:: With potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; for 8h; Ambient temperature;
DOI:10.1246/bcsj.69.1099

Reference yield: 97.0%

: 40162-66-1
Boc-Gln-Pro-OBzl*HCl

: H-Gln-Pro-OBzl*HCl

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; formic acid; at 0 ℃; for 0.5h;

Reference yield:

: 40162-66-1
Boc-Gln-Pro-OBzl*HCl

: H-Val-Val-Val-Pro-Pro-Phe-Leu-Gln-Pro-OH

Guidance literature:: Multi-step reaction with 8 steps

1: 97 percent / 4.5 N HCl / dioxane; formic acid / 0.5 h / 0 °C

2: 82 percent / NMM / dimethylformamide / Ambient temperature

3: 93 percent / 4.5 N HCL / dioxane; formic acid / 0.5 h / 0 °C

4: 60 percent / NMM / dimethylformamide / Ambient temperature

5: 95 percent / 4.5 N HCl / dioxane; formic acid / 30 h / 0 °C

6: 1.) 1 N sulfuric acid 2.) ECF, NMM / 1.) ethyl acetate 2.) THF, DMF, 0 deg C, 1 h than room temp.

7: 96 percent / 4.5 N HCl / dioxane; formic acid / 0.5 h / 0 °C

8: 90 percent / H₂ / Palladium black / acetic acid / 10 h

With 4-methyl-morpholine; hydrogenchloride; sulfuric acid; hydrogen; chloroformic acid ethyl ester; palladium; In 1,4-dioxane; formic acid; acetic acid; N,N-dimethyl-formamide;