methyl 9-(tert-butyldiphenylsilyloxy)-2-methylene-3-methoxycarbonylnonanate

Base Information

Chemical Name:methyl 9-(tert-butyldiphenylsilyloxy)-2-methylene-3-methoxycarbonylnonanate
CAS No.:1046480-15-2
Molecular Formula:C₂₉H₄₀O₅Si
Molecular Weight:496.719
Hs Code.:

Synonyms:methyl 9-(tert-butyldiphenylsilyloxy)-2-methylene-3-methoxycarbonylnonanate

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Chemical Property of methyl 9-(tert-butyldiphenylsilyloxy)-2-methylene-3-methoxycarbonylnonanate

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Technology Process of methyl 9-(tert-butyldiphenylsilyloxy)-2-methylene-3-methoxycarbonylnonanate

There total 1 articles about methyl 9-(tert-butyldiphenylsilyloxy)-2-methylene-3-methoxycarbonylnonanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 26805-54-9,61784-44-9,19530-68-8
dimethyl (Z)-2-(bromomethyl)fumarate

: 172995-33-4
((6-bromohexyl)oxy)(tert-butyl)diphenylsilane

: 1046480-15-2
methyl 9-(tert-butyldiphenylsilyloxy)-2-methylene-3-methoxycarbonylnonanate

Guidance literature:: ((6-bromohexyl)oxy)(tert-butyl)diphenylsilane; With iodine; magnesium; In diethyl ether; at 20 ℃; for 3h;

dimethyl (Z)-2-(bromomethyl)fumarate; In diethyl ether; at -78 ℃; for 19h; Further stages.;
DOI:10.1016/j.tet.2008.05.035