1,3-dicarbobenzoxy-2-hydroxybenzimidazoline

Base Information

• Chemical Name: 1,3-dicarbobenzoxy-2-hydroxybenzimidazoline
• CAS No.: 75144-33-1
• Molecular Formula: C₂₃H₂₀N₂O₅
• Molecular Weight: 404.422
• Mol file: 75144-33-1.mol

Synonyms:1,3-dicarbobenzoxy-2-hydroxybenzimidazoline

Chemical Property of 1,3-dicarbobenzoxy-2-hydroxybenzimidazoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-dicarbobenzoxy-2-hydroxybenzimidazoline

There total 2 articles about 1,3-dicarbobenzoxy-2-hydroxybenzimidazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

benzoimidazole (51-17-2,79351-71-6) + benzyl chloroformate (501-53-1,94274-21-2) → 1,3-dicarbobenzoxy-2-hydroxybenzimidazoline (75144-33-1)

Guidance literature:

In water; benzene;

DOI:10.1021/ja00542a020

Reference yield:

→ 1,3-dicarbobenzoxy-2-hydroxybenzimidazoline (75144-33-1)

Guidance literature:

N-Carbobenzoxy-2-hydroxy-benzimidazol, Carbobenzoxychlorid;

Reference yield:

1,3-dicarbobenzoxy-2-hydroxybenzimidazoline (75144-33-1) → N,N'-dicarbobenzoxy-N-formyl-1,2-diaminobenzene (75144-34-2)

Guidance literature:

With triethylamine; In acetonitrile;

DOI:10.1021/ja00542a020

upstream raw materials:

benzoimidazole

benzyl chloroformate

Downstream raw materials:

2-methoxy-benzimidazole-1,3-dicarboxylic acid dibenzyl ester

N,N'-dicarbobenzoxy-N-formyl-1,2-diaminobenzene