2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole

Base Information

Chemical Name:2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole
CAS No.:162687-83-4
Molecular Formula:C₂₆H₃₆N₄S
Molecular Weight:436.665
Hs Code.:

Synonyms:2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole

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Chemical Property of 2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole

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Technology Process of 2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole

There total 6 articles about 2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 162687-82-3
N-<2-(N',N'-diethylamino)ethyl>-5-<(4,5-diphenyl-1H-imidazol-2-yl)thio>pentanamide

: 162687-83-4
2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; for 4h; Heating;
DOI:10.1021/jm00007a004

Reference yield:

: 119-53-9,579-44-2
2-hydroxy-2-phenylacetophenone

: 162687-83-4
2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylformamide; various solvent(s) / 160 °C

2: K₂CO₃, tetra-n-butylammonium iodide / tetrahydrofuran / 2 h / Heating

3: NaOH

4: 1.) 1-hydroxybenzotriazole hydrate, 2.) dicyclohexylcarbodiimide / 1.) DMF, RT, 20 min, 2.) DMF, RT, 48 h

5: 99 percent / sodium bis(2-methoxyethoxy)aluminum hydride / toluene / 4 h / Heating

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00007a004

Reference yield:

: 130804-18-1
5-(4,5-diphenyl-1H-imidazol-2-ylthio)-pentanoic acid

: 162687-83-4
2-<<5-<<2-(N,N-diethylamino)ethyl>amino>pentyl>thio>-4,5-diphenyl-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1-hydroxybenzotriazole hydrate, 2.) dicyclohexylcarbodiimide / 1.) DMF, RT, 20 min, 2.) DMF, RT, 48 h

2: 99 percent / sodium bis(2-methoxyethoxy)aluminum hydride / toluene / 4 h / Heating

With 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene;
DOI:10.1021/jm00007a004