(S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester

Base Information

Chemical Name:(S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester
CAS No.:1005760-95-1
Molecular Formula:C₂₃H₃₂N₂O₈
Molecular Weight:464.516
Hs Code.:

Synonyms:(S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester

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Chemical Property of (S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester

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Technology Process of (S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester

There total 1 articles about (S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 123639-56-5
(S)-N-benzylserine methyl ester

: 132286-77-2
(S)-4-(allyloxy)-2-((tert-butoxycarbonyl)amino)-4-oxobutanoic acid

: 1005760-95-1
(S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; at 0 - 20 ℃; for 25h;
DOI:10.1021/jo702072z

Reference yield: 81.0%

: 1005760-95-1
(S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester

: 1005760-99-5
[(2S,5S)-4-benzyl-5-hydroxymethyl-3,6-dioxopiperazin-2-yl]acetic acid ally ester

Guidance literature:: (S)-N-benzyl-3-tert-butoxycarbonylamino-N-[(S)-2-hydroxy-1-methoxycarbonylethyl]succinamic acid ally ester; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In water; ethyl acetate; at 20 ℃; Further stages.;
DOI:10.1021/jo702072z