2,5-dichloro-β-phenethylsulfonyl azide

Base Information

Chemical Name:2,5-dichloro-β-phenethylsulfonyl azide
CAS No.:96129-69-0
Molecular Formula:C₈H₇Cl₂N₃O₂S
Molecular Weight:280.134
Hs Code.:

Synonyms:2,5-dichloro-β-phenethylsulfonyl azide

Suppliers and Price of 2,5-dichloro-β-phenethylsulfonyl azide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 3 raw suppliers

Chemical Property of 2,5-dichloro-β-phenethylsulfonyl azide

Chemical Property:

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Technology Process of 2,5-dichloro-β-phenethylsulfonyl azide

There total 4 articles about 2,5-dichloro-β-phenethylsulfonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.3%

: 96129-68-9
2,5-dichloro-β-phenethylsulfonyl chloride

: 96129-69-0
2,5-dichloro-β-phenethylsulfonyl azide

Guidance literature:: With sodium azide; In water; acetone; Ambient temperature;
DOI:10.1021/jo00212a013

Reference yield: 40.1%

: 96129-70-3
2,5-dichloro-β-phenethylsulfonamide

: 96129-69-0
2,5-dichloro-β-phenethylsulfonyl azide

Guidance literature:: In 1,1,2-Trichloro-1,2,2-trifluoroethane; at 185 ℃; for 24h;
DOI:10.1021/jo00212a013

Reference yield:

: 40173-98-6
2,5-dichloro-β-phenethyl bromide

: 96129-69-0
2,5-dichloro-β-phenethylsulfonyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / sodium sulfite / aq. ethanol; H₂O

2: 86.4 percent / SOCl₂ / benzene; dimethylformamide / Heating

3: 68.3 percent / NaN₃ / acetone; H₂O / Ambient temperature

With thionyl chloride; sodium azide; sodium sulfite; In ethanol; water; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/jo00212a013