4-chlorobezoin phenylacetate

Base Information

Chemical Name:4-chlorobezoin phenylacetate
CAS No.:108511-28-0
Molecular Formula:C₂₂H₁₇ClO₃
Molecular Weight:364.828
Hs Code.:

Synonyms:4-chlorobezoin phenylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chlorobezoin phenylacetate

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Technology Process of 4-chlorobezoin phenylacetate

There total 2 articles about 4-chlorobezoin phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1889-78-7
2-bromo-1-(4-chlorophenyl)-2-phenylethanone

: 13005-36-2
potassium phenylacetate

: 108511-28-0
4-chlorobezoin phenylacetate

Guidance literature:: With 18-crown-6 ether; In acetonitrile; for 2h; Heating;
DOI:10.1021/jo00389a034

Reference yield:

: 1889-71-0
4'-chloro-2-phenylacetophenone

: 108511-28-0
4-chlorobezoin phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / bromine / diethyl ether / 0.5 h

2: 55 percent / 18-crown-6 / acetonitrile / 2 h / Heating

With 18-crown-6 ether; bromine; In diethyl ether; acetonitrile;
DOI:10.1021/jo00389a034