bis(2,4,6-trichlorophenyl) n-pentylmalonate

Base Information

• Chemical Name: bis(2,4,6-trichlorophenyl) n-pentylmalonate
• CAS No.: 77517-83-0
• Molecular Formula: C₂₀H₁₆Cl₆O₄
• Molecular Weight: 533.063
• Mol file: 77517-83-0.mol

Synonyms:bis(2,4,6-trichlorophenyl) n-pentylmalonate

Chemical Property of bis(2,4,6-trichlorophenyl) n-pentylmalonate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of bis(2,4,6-trichlorophenyl) n-pentylmalonate

There total 2 articles about bis(2,4,6-trichlorophenyl) n-pentylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-n-pentyl malonic acid (616-88-6) + 2,4,6-Trichlorophenol (88-06-2,67471-29-8) → bis(2,4,6-trichlorophenyl) n-pentylmalonate (77517-83-0)

Guidance literature:

With trichlorophosphate; at 80 ℃; for 7h;

DOI:10.1021/jm00138a002

Reference yield:

diethyl n-pentylmalonate (6065-59-4) → bis(2,4,6-trichlorophenyl) n-pentylmalonate (77517-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / KOH / H₂O / 3 h / 90 °C

2: 84 percent / POCl₃ / 7 h / 80 °C

With potassium hydroxide; trichlorophosphate; In water;

DOI:10.1021/jm00138a002

upstream raw materials:

2-n-pentyl malonic acid

2,4,6-Trichlorophenol

diethyl n-pentylmalonate

Refernces