5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride

Base Information

• Chemical Name: 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride
• CAS No.: 949167-04-8
• Molecular Formula: C₁₁H₁₂ClF₃N₂O*ClH
• Molecular Weight: 317.138

Synonyms:5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride

Chemical Property of 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride

There total 1 articles about 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl N'-[5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate (949166-95-4) → 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride (949167-04-8)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 1h;

Reference yield:

(E)-3-[2-fluoro-5-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acrylic acid (949167-21-9) + 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride (949167-04-8) → 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid N'-{(E)-3-[2-fluoro-5-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acryloyl}hydrazide (949167-22-0)

Guidance literature:

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

(Z)-2-fluoro-3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acrylic acid (870838-71-4) + 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid hydrazide hydrochloride (949167-04-8) → 5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid N'-{(Z)-2-fluoro-3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acryloyl}hydrazide (949167-05-9)

Guidance literature:

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 13h;

upstream raw materials:

tert-butyl N'-[5-chloro-2-(3,4,5-trifluorophenyl)pentanoyl]hydrazinecarboxylate

Downstream raw materials:

5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid N'-{(Z)-2-fluoro-3-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acryloyl}hydrazide

5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid N'-{(E)-3-[3-fluoro-4-(4-methyl-1H-imidazol-1-yl)phenyl]acryloyl}hydrazide

5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid N'-{(E)-3-[2-fluoro-5-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]acryloyl}hydrazide

5-chloro-2-(3,4,5-trifluorophenyl)pentanoic acid N'-{(E)-3-[5-methoxy-6-(4-methyl-1H-imidazol-1-yl)pyridin-3-yl]acryloyl}hydrazide

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