Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester

Base Information

• Chemical Name: Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester
• CAS No.: 737805-74-2
• Molecular Formula: C₂₆H₂₄INO₂
• Molecular Weight: 509.387

Synonyms:Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester

Chemical Property of Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester

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Technology Process of Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester

There total 1 articles about Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (R)-1-[(S)-1-(9-phenyl-9H-fluoren-9-ylamino)-ethyl]-allyl ester → Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester (737805-74-2) + Acetic acid (2S,3S,4R)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester

Guidance literature:

With iodine; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; at 20 ℃; for 18h;

DOI:10.1021/ol049237g

Reference yield: 97.0%

Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester (737805-74-2) → (2S,3S,4S)-2-methyl-3,4-dihydroxy-N-(9-phenylfluoren-9-yl)pyrrolidine + (2S,3S,4R)-2-methyl-3,4-dihydroxy-N-(9-phenylfluoren-9-yl)pyrrolidine

Guidance literature:

Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester; With silver(I) acetate; In toluene; for 3h; Heating;

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/ol049237g

Reference yield:

Acetic acid (2S,3S,4S)-4-iodo-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester (737805-74-2) → Acetic acid (3R,4S,5S)-4-hydroxy-5-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester + Acetic acid (2S,3S,4R)-4-hydroxy-2-methyl-1-(9-phenyl-9H-fluoren-9-yl)-pyrrolidin-3-yl ester

Guidance literature:

With silver tetrafluoroborate; water; In toluene; at 20 ℃; for 12h; Title compound not separated from byproducts;

DOI:10.1021/ol049237g

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