[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

Base Information

Chemical Name:[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride
CAS No.:643063-86-9
Molecular Formula:C₁₈H₁₃ClN₂O₂Pt
Molecular Weight:519.846
Hs Code.:

Synonyms:[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

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Chemical Property of [4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

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Technology Process of [4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

There total 1 articles about [4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51329-15-8
methyl 3,5-dibromobenzoate

: 643063-86-9
[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene / 8 h / 140 °C / Inert atmosphere; Sealed tube; Sonication; Microwave irradiation

2: triphenylphosphine; sodium carbonate; palladium diacetate / tetrahydrofuran; water / 85 °C / Inert atmosphere

3: water; acetonitrile / 72 h / Inert atmosphere; Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium diacetate; sodium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; water; toluene; acetonitrile;
DOI:10.1016/j.ejmech.2017.09.058

Reference yield: 92.0%

: 643063-86-9
[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

: 1849-36-1
para-nitrobenzenethiol

: 1610038-03-3
Pt(1,3-bis(2-pyridyl)-benzene)(4-nitrothiophenolate)

Guidance literature:: para-nitrobenzenethiol; With potassium tert-butylate; In methanol; Inert atmosphere;

[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride; In methanol; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ic500555w

Reference yield: 81.0%

: 643063-86-9
[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

: 108-98-5
thiophenol

: 1610038-00-0
Pt(1,3-bis(2-pyridyl)-benzene)(thiophenolate)

Guidance literature:: thiophenol; With potassium tert-butylate; In methanol; Inert atmosphere;

[4-(methoxycarbonyl)-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride; In methanol; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ic500555w