(5S,9S,10S)-t-butyl 13-azalabda-8⁽¹⁷⁾-en-15-oate

Base Information

• Chemical Name: (5S,9S,10S)-t-butyl 13-azalabda-8⁽¹⁷⁾-en-15-oate
• CAS No.: 369363-40-6
• Molecular Formula: C₂₃H₄₁NO₂
• Molecular Weight: 363.584

Synonyms:(5S,9S,10S)-t-butyl 13-azalabda-8⁽¹⁷⁾-en-15-oate

Chemical Property of (5S,9S,10S)-t-butyl 13-azalabda-8⁽¹⁷⁾-en-15-oate

Chemical Property:

Purity/Quality:

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Technology Process of (5S,9S,10S)-t-butyl 13-azalabda-8⁽¹⁷⁾-en-15-oate

There total 1 articles about (5S,9S,10S)-t-butyl 13-azalabda-8⁽¹⁷⁾-en-15-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

manool (596-85-0) → (5S,9S,10S)-t-butyl 13-azalabda-8(17)-en-15-oate (369363-40-6)

Guidance literature:

Multi-step reaction with 6 steps

1: pyridinium chlorochromate / CH₂Cl₂ / 18 h

2: K₂CO₃ / tetrahydrofuran; H₂O / 48 h / Heating

3: I₂; KOH; KI / dioxane; H₂O / 2 h

4: diphenylphosphoryl azide; triethylamine / benzene / 3.5 h / Heating

5: LiAlH₄ / tetrahydrofuran / 2 h / Heating

6: Et₃N / tetrahydrofuran / 1 h / 0 °C

With potassium hydroxide; lithium aluminium tetrahydride; diphenylphosphoranyl azide; iodine; potassium carbonate; triethylamine; pyridinium chlorochromate; potassium iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; benzene; 4: Curtius rearrangement;

DOI:10.1021/ja010670k

upstream raw materials:

manool

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